1-乙烯基-7-氧杂双环[4.1.0]庚-2,4-二烯合成路线 （共 6 条）
反应条件
potassium tert-butylate in diethyl ether
T=-20°C; 0.5 h; Yield given;
参考文献
Watanabe, Tadashi; Hiratsuka, Akira; Aizawa, Toshiko; Sawahata, Tadashi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1185 - 1188
反应条件
1: 1.) Br2, 2.) PBr3 / 1.) CCl4, MeOH 2.) CCl4, 0 deg C
2: perbenzoic acid / CHCl3
3: tBuOK / diethyl ether / 0.5 h / -20 °C
View Scheme
参考文献
Watanabe, Tadashi; Hiratsuka, Akira; Aizawa, Toshiko; Sawahata, Tadashi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1185 - 1188
反应条件
1: perbenzoic acid / CHCl3
2: Br2 / CCl4 / -20 °C
3: tBuOK / diethyl ether / 0.5 h / -20 °C
View Scheme
参考文献
Watanabe, Tadashi; Hiratsuka, Akira; Aizawa, Toshiko; Sawahata, Tadashi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1185 - 1188
反应条件
1: Br2 / CCl4 / -20 °C
2: tBuOK / diethyl ether / 0.5 h / -20 °C
View Scheme
参考文献
Watanabe, Tadashi; Hiratsuka, Akira; Aizawa, Toshiko; Sawahata, Tadashi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1185 - 1188
反应条件
1: perbenzoic acid / CHCl3
2: tBuOK / diethyl ether / 0.5 h / -20 °C
View Scheme
参考文献
Watanabe, Tadashi; Hiratsuka, Akira; Aizawa, Toshiko; Sawahata, Tadashi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1185 - 1188
反应条件
1: LiBr / acetone / Heating
2: perbenzoic acid / CHCl3
3: Br2 / CCl4 / -20 °C
4: tBuOK / diethyl ether / 0.5 h / -20 °C
View Scheme
参考文献
Watanabe, Tadashi; Hiratsuka, Akira; Aizawa, Toshiko; Sawahata, Tadashi
Tetrahedron Letters, 1982 , vol. 23, # 11 p. 1185 - 1188
