您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
盐酸特比萘芬
合成路线
（共 16 条）
14489-75-9
N-甲基-1-萘甲氨
+
78629-20-6
3-羟基-6,6-二甲基-1-庚烯-4-炔
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
1: 3-hydroxy-6,6-dimethylhept-1-ene-4-yne With hydrogenchloride; trichlorophosphate in methanol T=0 - 20°C; 20 - 24 h; 2: N-methyl-N-(1-naphthyl)methyl amine With sodium hydroxide T=80°C; 3: With hydrogenchloride in dichloromethane; water T=20°C;
参考文献
HYDEX CHEMICALS PVT LTD.
Patent: WO2005/110968 A1, 2005 ;
Location in patent: Page/Page column 9-10 ;
91161-71-6
特比萘芬
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
hydrogenchloride in water; butanone T=20 - 30°C; 0.25 h;
参考文献
F.I.S. FABBRICA ITALIANA SINTETICI S.P.A.; DELLA NEGRA, Frederico
Patent: WO2005/121155 A1, 2005 ;
Location in patent: Page/Page column 37-38 ;
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
sodium hydroxide; sodium borohydride in ethyl acetate; isopropyl alcohol; toluene
参考文献
Lee, Tai-Au; Wang, Kyu-Jung; Kim, Hong-Bae; Kwon, Kyoung-Chan; Ku, Chang-Hoe
Patent: US2003/130530 A1, 2003 ;
126764-17-8
6,6-二甲基-2-烯-4-炔氯代庚烷
+
14489-75-9
N-甲基-1-萘甲氨
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
1: With sodium hydroxide in water T=20 - 100°C; 2 h; 2: With hydrogenchloride in dichloromethane; water T=20°C; 1 h;
参考文献
WO2007/52089 A1, ;
Page/Page column 7 ;
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
sodium hydroxide; sodium borohydride; acetic acid in ethyl acetate; toluene; tert-butyl alcohol
参考文献
Lee, Tai-Au; Wang, Kyu-Jung; Kim, Hong-Bae; Kwon, Kyoung-Chan; Ku, Chang-Hoe
Patent: US2003/130530 A1, 2003 ;
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
sodium hydroxide; sodium borohydride in ethyl acetate; isopropyl alcohol; toluene
参考文献
Lee, Tai-Au; Wang, Kyu-Jung; Kim, Hong-Bae; Kwon, Kyoung-Chan; Ku, Chang-Hoe
Patent: US2003/130530 A1, 2003 ;
65473-13-4
N-甲基-1-萘甲胺盐酸盐
+
287471-30-1
1-氯-6,6-二甲基-2-庚烯-4-炔
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
1: With potassium carbonate in dimethyl sulfoxide T=25 - 60°C; 4.25 - 6.5 h; 2: With hydrogenchloride in water; ethyl acetate T=0 - 10°C; pH=1.5 - 2; 0.5 h; Product distribution / selectivity;
参考文献
US2006/84826 A1, ;
Page/Page column 3 ;
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
sodium hydroxide; sodium borohydride in methanol; ethyl acetate; toluene
参考文献
Lee, Tai-Au; Wang, Kyu-Jung; Kim, Hong-Bae; Kwon, Kyoung-Chan; Ku, Chang-Hoe
Patent: US2003/130530 A1, 2003 ;
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
sodium hydroxide; sodium borohydride in ethyl acetate; isopropyl alcohol; toluene
参考文献
Lee, Tai-Au; Wang, Kyu-Jung; Kim, Hong-Bae; Kwon, Kyoung-Chan; Ku, Chang-Hoe
Patent: US2003/130530 A1, 2003 ;
→
反应条件
78628-80-5
盐酸特比萘芬
反应条件
sodium hydroxide; sodium borohydride in ethyl acetate; isopropyl alcohol; toluene
参考文献
Lee, Tai-Au; Wang, Kyu-Jung; Kim, Hong-Bae; Kwon, Kyoung-Chan; Ku, Chang-Hoe
Patent: US2003/130530 A1, 2003 ;
1
2
下一页
末页
到第
页
确定
