2-甲基庚-6-烯-3-醇合成路线 （共 6 条）
反应条件
1: 4-bromo-but-1-ene With magnesium in diethyl ether
Heating;
2: isobutyraldehyde in diethyl ether
Heating; Further stages.;
参考文献
Taillier, Catherine; Hameury, Thomas; Bellosta, Veronique; Cossy, Janine
Tetrahedron, 2007 , vol. 63, # 21 p. 4472 - 4490
反应条件
1: (chloromethyl)-cyclopropane With naphthalene; lithium in diethyl ether
T=0°C; 1 h;
2: isobutyraldehyde in diethyl ether
T=0°C; 0.5 h;
参考文献
Penafiel, Itziar; Pastor, Isidro M.; Yus, Miguel
Tetrahedron, 2010 , vol. 66, # 16 p. 2928 - 2935
反应条件
ammonium acetate; sodium cyanoborohydride in methanol
T=23°C;
参考文献
Zabawa, Thomas P.; Chemler, Sherry R.
Organic Letters, 2007 , vol. 9, # 10 p. 2035 - 2038
反应条件
dichloro-(phenyl)borane; potassium carbonate in dichloromethane
T=20°C; 14 h; Inert atmosphere; regioselective reaction;
参考文献
Pei, Wenbo; Krauss, Isaac J.
Journal of the American Chemical Society, 2011 , vol. 133, # 46 p. 18514 - 18517
反应条件
in tetrahydrofuran
T=-30°C; 1 h;
参考文献
Molander, Gary A.; McKie, Jeffrey A.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3186 - 3192
反应条件
in tetrahydrofuran
T=-50 - 20°C; Inert atmosphere;
参考文献
Nahra, Fady; Liron, Frederic; Prestat, Guillaume; Mealli, Carlo; Messaoudi, Abdelatif; Poli, Giovanni
Chemistry - A European Journal, 2009 , vol. 15, # 42 p. 11078 - 11082
