4-乙氧羰基硫杂环戊-3-酮合成路线 （共 11 条）
反应条件
sodium ethanolate in toluene
Heating;
参考文献
DUUS, F.
Tetrahedron, 1981 , vol. 37, # 15 p. 2633 - 2640
反应条件
sodium ethanolate in ethanol
T=0°C; Yields of byproduct given;
参考文献
DUUS, F.
Tetrahedron, 1981 , vol. 37, # 15 p. 2633 - 2640
反应条件
sodium hydride in tetrahydrofuran
Ambient temperature;
参考文献
Yamada, Yasuji; Ishii, Toshihide; Kimura, Masayuki; Hosaka, Kunio
Tetrahedron Letters, 1981 , vol. 22, # 14 p. 1353 - 1354
反应条件
1: piperidine
2: sodium; benzene
View Scheme
参考文献
Buchman; Cohen
Journal of the American Chemical Society, 1944 , vol. 66, p. 847
反应条件
1: tetrahydrofuran / Ambient temperature
2: 70 percent / sodium hydride / tetrahydrofuran / Ambient temperature
View Scheme
参考文献
Yamada, Yasuji; Ishii, Toshihide; Kimura, Masayuki; Hosaka, Kunio
Tetrahedron Letters, 1981 , vol. 22, # 14 p. 1353 - 1354
反应条件
sodium ethanolate
16 h; Heating;
参考文献
Shinkwin, Anne E.; Whish, William J. D.; Threadgill, Michael D.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 2 p. 297 - 308
反应条件
sodium ethanolate; benzene
参考文献
Brown et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 155,158
反应条件
1: 33 percent / toluene / 3 h / Heating
2: 86 percent / N-Chlorosuccinimide / pyridine / 0.33 h / Heating
3: 94 percent / Phosphorus pentasulfide / pyridine / 4 h / Heating
4: 60 percent / Sodium ethoxide / ethanol
View Scheme
参考文献
Press; Hofmann; Wiegand; Safir
Journal of Heterocyclic Chemistry, 1982 , vol. 19, # 2 p. 391 - 413
反应条件
in toluene
3 h; Heating; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Press; Hofmann; Wiegand; Safir
Journal of Heterocyclic Chemistry, 1982 , vol. 19, # 2 p. 391 - 413
反应条件
ethanol; sodium ethanolate
Behandeln des Reaktionsprodukts mit wss. Schwefelsaeure.;
参考文献
Karrer; Schmid
Helvetica Chimica Acta, 1944 , vol. 27, p. 124,126
