lithium aluminium tetrahydride in diethyl ether 3 h; Ambient temperature;

1: 1.) hydrogen chloride gas, 2.) water / 1.) ether, 45 min, 2.) 40 deg C 2: 92 percent / potassium carbonate / acetone / 5 h / Heating 3: 78 percent / lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature View Scheme

1: 92 percent / potassium carbonate / acetone / 5 h / Heating 2: 78 percent / lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature View Scheme