5-[[4-[4-(2,2-二苯基乙烯基)苯基]-1,2,3,3a,4,8b-六氢环戊烯并[b]吲哚-7-基]亚甲基]-2-(3-乙基-4-氧代-2-硫酮-5-噻唑亚基)-4-氧代-3-噻唑烷乙酸合成路线 (共 6 条)
反应条件
1.1: sodium tetrahydroborate; acetic acid / 20 °C 2.1: tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate / anhydrous xylene / 120 °C 3.1: trichlorophosphate / 10 °C 3.2: 20 °C 4.1: ammonium acetate; acetic acid / 120 °C View Scheme
参考文献
Dyes and Pigments, , vol. 91, # 2 p. 145 - 152
反应条件
1.1: tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate / anhydrous xylene / 120 °C 2.1: trichlorophosphate / 10 °C 2.2: 20 °C 3.1: ammonium acetate; acetic acid / 120 °C View Scheme
参考文献
Dyes and Pigments, , vol. 91, # 2 p. 145 - 152
反应条件
1.1: sodium acetate; acetic acid / dichloromethane; water / 2 h / Reflux 2.1: sodium tetrahydroborate; acetic acid / 20 °C 3.1: tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate / anhydrous xylene / 120 °C 4.1: trichlorophosphate / 10 °C 4.2: 20 °C 5.1: ammonium acetate; acetic acid / 120 °C View Scheme
参考文献
Dyes and Pigments, , vol. 91, # 2 p. 145 - 152
反应条件
1.1: sodium acetate; acetic acid / dichloromethane; water / 2 h / Reflux 2.1: sodium tetrahydroborate; acetic acid / 20 °C 3.1: tri-tert-butyl phosphine; potassium tert-butylate; palladium diacetate / anhydrous xylene / 120 °C 4.1: trichlorophosphate / 10 °C 4.2: 20 °C 5.1: ammonium acetate; acetic acid / 120 °C View Scheme
参考文献
Dyes and Pigments, , vol. 91, # 2 p. 145 - 152
反应条件
ammonium acetate; acetic acid T=120°C;
参考文献
Dyes and Pigments, , vol. 91, # 2 p. 145 - 152
反应条件
1.1: trichlorophosphate / 10 °C 1.2: 20 °C 2.1: ammonium acetate; acetic acid / 120 °C View Scheme
参考文献
Dyes and Pigments, , vol. 91, # 2 p. 145 - 152