3,6,9,15-四氮杂双环[9.3.1]十五碳-1(15),11,13-三烯合成路线 （共 5 条）
反应条件
sodium carbonate; thiophenol in N,N-dimethyl-formamide
T=20°C;
参考文献
Siaugue, Jean-Michel; Segat-Dioury, Fabienne; Sylvestre, Isabelle; Favre-Reguillon, Alain; Foos, Jacques; Madic, Charles; Guy, Alain
Tetrahedron, 2001 , vol. 57, # 22 p. 4713 - 4718
反应条件
1: 87 percent / Na2CO3 / dimethylformamide / 100 °C
2: 72 percent / Na2CO3; PhSH / dimethylformamide / 20 °C
View Scheme
参考文献
Siaugue, Jean-Michel; Segat-Dioury, Fabienne; Sylvestre, Isabelle; Favre-Reguillon, Alain; Foos, Jacques; Madic, Charles; Guy, Alain
Tetrahedron, 2001 , vol. 57, # 22 p. 4713 - 4718
反应条件
hydrogen bromide; acetic acid
参考文献
Wen, Jinghan; Geng, Zhirong; Yin, Yuxin; Wang, Zhilin
Inorganic Chemistry Communications, 2012 , vol. 21, p. 16 - 20
反应条件
1: sulfuric acid; hydrogen bromide
2: potassium carbonate / N,N-dimethyl-formamide
3: hydrogen bromide; acetic acid
View Scheme
参考文献
Wen, Jinghan; Geng, Zhirong; Yin, Yuxin; Wang, Zhilin
Inorganic Chemistry Communications, 2012 , vol. 21, p. 16 - 20
反应条件
1: 82 percent / Bu4N(HSO4); aq. 50 percent NaOH / toluene / Heating
2: 75 percent / HCl gas; NaOH / dioxane / 20 °C
View Scheme
参考文献
Chellini, Andrea; Pagliarin, Roberto; Giovenzanna, Giovanni B.; Palmisano, Giovanni; Sisti, Massimo
Helvetica Chimica Acta, 2000 , vol. 83, # 4 p. 793 - 800
