4-氨基-N-(2-甲氧基苯基)-苯甲酰胺合成路线 （共 5 条）
反应条件
10 palladium on activated charcoal; hydrogen in ethanol
T=20°C; 16 h;
参考文献
Cashman, John; Lanier, Marion; Mercola, Mark; Schade, Dennis; Willems, Erik
Patent: US2013/177535 A1, 2013 ;
Location in patent: Paragraph 0176 ;
反应条件
1: pyridine / 3 h / Reflux
2: 10 palladium on activated charcoal; hydrogen / ethanol / 16 h / 20 °C
View Scheme
参考文献
Lanier, Marion; Schade, Dennis; Willems, Erik; Tsuda, Masanao; Spiering, Sean; Kalisiak, Jaroslaw; Mercola, Mark; Cashman, John R.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 2 p. 697 - 708
反应条件
1: pyridine / 3 h / Reflux
2: 10 palladium on activated charcoal; hydrogen / ethanol / 16 h / 20 °C
View Scheme
参考文献
Lanier, Marion; Schade, Dennis; Willems, Erik; Tsuda, Masanao; Spiering, Sean; Kalisiak, Jaroslaw; Mercola, Mark; Cashman, John R.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 2 p. 697 - 708
反应条件
1: thionyl chloride / 2 h / Reflux
2: pyridine / 3 h / Reflux
3: 10 palladium on activated charcoal; hydrogen / ethanol / 16 h / 20 °C
View Scheme
参考文献
Lanier, Marion; Schade, Dennis; Willems, Erik; Tsuda, Masanao; Spiering, Sean; Kalisiak, Jaroslaw; Mercola, Mark; Cashman, John R.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 2 p. 697 - 708
反应条件
1.1: thionyl chloride / 2 h / |Reflux
1.2: |Reflux
2.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C
View Scheme
参考文献
Cashman, John; Lanier, Marion; Mercola, Mark; Schade, Dennis; Willems, Erik
Patent: US2013/177535 A1, 2013 ;
