四乙基二氟亚甲基二膦酸酯合成路线 （共 20 条）
反应条件
1: 12 h / Ambient temperature; Irradiation; in a quartz Rotaflo tube, 254 nm
2: Me3COOH / methanol; dimethylformamide / 0.5 h / -20 °C
View Scheme
参考文献
Nair, Haridasan K.; Burton, Donald J.
Tetrahedron Letters, 1995 , vol. 36, # 3 p. 347 - 350
反应条件
1: LDA / tetrahydrofuran / -78 °C
2: 74 percent / tetrahydrofuran
View Scheme
参考文献
Obayashi, Michio; Ito, Eiji; Matsui, Kiyohide; Kondo, Kiyosi
Tetrahedron Letters, 1982 , vol. 23, # 22 p. 2323 - 2326
反应条件
lithium diisopropyl amide in tetrahydrofuran
1.) -78 deg C, 30 min, 2.) -78 deg C, 30 min; -78 to 0 deg C;
参考文献
Shipitsin, Alexander V.; Victorova, Lyubov S.; Shirokova, Elena A.; Dyatkina, Natalya B.; Goryunova, Lyudmila E.; Beabealashvilli, Robert Sh; Hamilton, Cliris J.; Roberts, Stanley M.; Krayevsky, Alexander
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 1039 - 1050
反应条件
lithium diisopropyl amide in tetrahydrofuran
1.) -78 deg C, 30 min, 2.) -78 to 0 deg C; Title compound not separated from byproducts;
参考文献
Shipitsin, Alexander V.; Victorova, Lyubov S.; Shirokova, Elena A.; Dyatkina, Natalya B.; Goryunova, Lyudmila E.; Beabealashvilli, Robert Sh; Hamilton, Cliris J.; Roberts, Stanley M.; Krayevsky, Alexander
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 1039 - 1050
反应条件
in toluene
1.) -5 deg C, 1 h, 2.) r.t.,;
参考文献
Blackburn, G. Michael; Taylor, Graham E.
Journal of Organometallic Chemistry, 1988 , vol. 348, p. 55 - 62
反应条件
perchloryl fluoride; potassium tert-butylate in toluene
0.833333 h; temperature below 22 deg C;
参考文献
McKenna, Charles E.; Shen, Pei-de
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4573 - 4576
参考文献
Burton,D.J.; Ishihara,T.
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 121
参考文献
Burton,D.J.; Ishihara,T.
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 121
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide
Substitution;
参考文献
Laux; Perigaud; Imbach; Gosselin
Nucleosides and Nucleotides, 1999 , vol. 18, # 4-5 p. 1003 - 1004
参考文献
Burton, Donald J.; Flynn, Richard M.
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 263 - 266
