(S)-(+)-4,5-二氢-2-苯基-4-噁唑羧酸甲酯合成路线 （共 17 条）
反应条件
triethylamine in dichloromethane T=20°C; 12 h;
参考文献
Mantilli, Luca; Mazet, Clement
Chemical Communications, 2010 , vol. 46, # 3 p. 445 - 447
反应条件
diethylamino-sulfur trifluoride in dichloromethane T=-78°C; 1 h;
参考文献
Jones, Geraint; Richards, Christopher J.
Tetrahedron Asymmetry, 2004 , vol. 15, # 4 p. 653 - 664
反应条件
1: benzamide With triethyloxonium tetra-fluoroborate in 1,2-dichloro-ethane T=20°C; 48 h; 2: With sodium carbonate in water 3: (l)-serine methyl ester hydrochloride in 1,2-dichloro-ethane 20 h; Heating;
参考文献
Glorius, Frank; Pfaltz, Andreas
Organic Letters, 1999 , vol. 1, # 1 p. 141 - 144
反应条件
Xtalfluor-E® in 1,2-dichloro-ethane T=90°C; 18 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 53, # 32 p. 4121 - 4123
反应条件
in 1,2-dichloro-ethane 20 h; Heating;
参考文献
Meyers; Schmidt; McKennon
Synthesis, 1993 , # 2 p. 250 - 262
反应条件
triethylamine in dichloromethane T=20°C; 2 h;
参考文献
Fukuhara, Tsuyoshi; Hasegawa, Chihiro; Hara, Shoji
Synthesis, 2007 , # 10 p. 1528 - 1534
反应条件
triethylamine in dichloromethane Ambient temperature;
参考文献
Reider; Eichen Conn; Davis; et al.
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3326 - 3334
反应条件
[Ru(η4-COD)(η3-methylallyl)2]; (S,S)-(R,R)-PhTRAP; hydrogen; N,N,N',N'-tetramethylguanidine in 2-methyl-propan-1-ol T=80°C; P=38002.6 Torr; 4 h; Autoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 133, # 19 p. 7312 - 7315
反应条件
1: 90 percent / HCl(g) / CH2Cl2 / 5 h 2: 65 percent / Et3N / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 15 p. 3326 - 3334
反应条件
1.1: oxalyl chloride / CH2Cl2 / 2 h / 40 °C 1.2: 76 percent / Et3N*3HF; Et3N / CH2Cl2 / 2 h / 20 °C 2.1: 86 percent / Et3N / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Synthesis, , # 10 p. 1528 - 1534
