2,3-二氢-3-碘甲基苯并呋喃合成路线 (共 4 条)
反应条件
1: With indium; iodine in N,N-dimethyl-formamide
T=20°C; 4 h;
2: With dihydrogen peroxide in N,N-dimethyl-formamide
T=20°C; 0.333333 h; Further stages.;
参考文献
Yanada, Reiko; Obika, Shingo; Nishimori, Nobuaki; Yamauchi, Masashige; Takemoto, Yoshiji
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2331 - 2334
反应条件
sodium iodide in acetone
0.5 h; Heating;
参考文献
Bhandal, Harcharan; Patel, Vinod F.; Pattenden, Gerald; Russell, Jamie J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 10 p. 2691 - 2701
反应条件
1: 99 percent / K2CO3 / dimethylformamide / 24 h / 25 °C
2: 1.) SmI2, HMPA, 2.) I2 / 1.) THF, 25 deg C, 5 min, 2.) THF, 25 deg C, 30 - 40 min
View Scheme
参考文献
Curran, Dennis P.; Totleben, Michael J.
Journal of the American Chemical Society, 1992 , vol. 114, # 15 p. 6050 - 6058
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
Heating;
参考文献
Beckwith, Athelstan L. J.; Meijs, Gordon F.
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 1922 - 1930