2,2'-亚甲基双(4,4,5,5-四甲基-1,3,2-二氧杂戊硼烷)合成路线 （共 23 条）
反应条件
1: With Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=20°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere; 2: With potassium hydroxide in 1,4-dioxane; water T=60°C; Suzuki-Miyaura Coupling; 6.5 h; Inert atmosphere;
参考文献
Endo, Kohei; Ishioka, Takafumi; Ohkubo, Takahiro; Shibata, Takanori
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7223 - 7231
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=25°C; Suzuki-Miyaura coupling; 5 h; Inert atmosphere; chemoselective reaction;
参考文献
Endo, Kohei; Ohkubo, Takahiro; Shibata, Takanori
Organic Letters, 2011 , vol. 13, # 13 p. 3368 - 3371
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=60°C; Suzuki-Miyaura Coupling; 5 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 17 p. 7223 - 7231
反应条件
1: With Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=20°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere; 2: With potassium hydroxide in 1,4-dioxane; water T=60°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Endo, Kohei; Ishioka, Takafumi; Ohkubo, Takahiro; Shibata, Takanori
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7223 - 7231
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=60°C; Suzuki-Miyaura Coupling; 5 h; Inert atmosphere;
参考文献
Endo, Kohei; Ishioka, Takafumi; Ohkubo, Takahiro; Shibata, Takanori
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7223 - 7231
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=25°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere; chemoselective reaction;
参考文献
Endo, Kohei; Ohkubo, Takahiro; Shibata, Takanori
Organic Letters, 2011 , vol. 13, # 13 p. 3368 - 3371
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=25°C; Suzuki-Miyaura coupling; 2 h; Inert atmosphere; chemoselective reaction;
参考文献
Endo, Kohei; Ohkubo, Takahiro; Shibata, Takanori
Organic Letters, 2011 , vol. 13, # 13 p. 3368 - 3371
反应条件
1: With Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=20°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere; 2: With potassium hydroxide in 1,4-dioxane; water T=60°C; Suzuki-Miyaura Coupling; 4 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 17 p. 7223 - 7231
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=20°C; Suzuki-Miyaura Coupling; 2 h; Time; chemoselective reaction;
参考文献
Endo, Kohei; Kurosawa, Fumiya; Ukaji, Yutaka
Chemistry Letters, 2013 , vol. 42, # 11 p. 1363 - 1365
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=20°C; Suzuki coupling; 2.5 h; Inert atmosphere; chemoselective reaction;
参考文献
Endo, Kohei; Ohkubo, Takahiro; Ishioka, Takafumi; Shibata, Takanori
Journal of Organic Chemistry, 2012 , vol. 77, # 10 p. 4826 - 4831
