Schwartz's reagent T=20°C;

C27H19N2(1+)*Cl(1-); 1,8-diazabicyclo[5.4.0]undec-7-ene in methanol T=20°C; 24 h; regioselective reaction;

C52H67Br2MoN2O2Si in benzene T=22°C; Cross Metathesis; P=100 Torr; 4 h; Glovebox; stereoselective reaction;

[(2,6-(2,4,6-Me3-C6H2-NdCMe)2C5H3N)Fe(N2)]2(μ2-N2) in neat (no solvent) T=25°C; Inert atmosphere;

1: phenylacetylene With [RhCl(η2:η2-cycloocta-1,5-diene)]2; benzo[1,3,2]dioxaborole in cyclohexane T=20°C; hydroboration; 2 h; 2: 2,3-dimethylbutane-2,3-diol Substitution; Title compound not separated from byproducts;

methanol; [(N,N′-bis[2,6-diisopropylphenyl]imidazolin-2-ylidene)CuCl]; sodium t-butanolate in tetrahydrofuran T=-15°C; 24 h; Inert atmosphere; regioselective reaction;

triethylamine; Rh olefin complex ligated to 1,3-dimethyl-imidazolylidene in tetrahydrofuran T=25°C; 14 h; Title compound not separated from byproducts.;

[RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,4-di(diphenylphosphino)-butane in 1,2-dichloro-ethane T=20°C; Hydroboration reaction; 24 h; regioselective reaction;

1: 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane With 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; copper(l) chloride; sodium t-butanolate in tetrahydrofuran T=20°C; 0.0833333 h; Inert atmosphere; 2: phenylacetylene; methyl iodide in tetrahydrofuran T=20°C; 16 h; Inert atmosphere; Reagent/catalyst; stereoselective reaction;

methanol; tri-tert-butyl phosphine; copper dichloride; sodium t-butanolate in toluene T=0 - 20°C; 2 h; Inert atmosphere; Overall yield = 78 percent; Overall yield = 50.1 mg; regioselective reaction;