6-吡啶-2-基吡啶-2-硫代甲酰胺合成路线 （共 3 条）
反应条件
hydrogen sulfide; triethylamine in ethanol
参考文献
Riis-Johannessen; Harding, Lindsay P.; Jeffery, John. C.; Moon, Ryan; Rice, Craig R.
Dalton Transactions, 2007 , # 16 p. 1577 - 1587
反应条件
1: benzoyl chloride / CH2Cl2 / Heating
2: 85 percent / g. H2S; triethylamine / ethanol
View Scheme
参考文献
Riis-Johannessen; Harding, Lindsay P.; Jeffery, John. C.; Moon, Ryan; Rice, Craig R.
Dalton Transactions, 2007 , # 16 p. 1577 - 1587
反应条件
1: 48.4 percent / 36percent H2O2 / acetic acid / 3 h / 85 °C
2: 62.4 percent / benzoyl chloride / H2O / Ambient temperature
3: 67.3 percent / ammonia, hydrogen sulfide / ethanol
View Scheme
参考文献
Antonini, Ippolito; Claudi, Francesco; Cristalli, Gloria; Franchetti, Palmarisa; Grifantini, Mario; Martelli, Sante
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1181 - 1184
