反应条件
1: 63 percent / tetrahydrofuran / 1.) -78 deg C to r.t., 2 h, 2.) r.t., 2 h
2: 1.) NaH / 1.) THF, r.t., 0.5 h, 2.) reflux, 3 h
3: 80 percent / 30percent aq. H2O2 / CH2Cl2 / or m-chloroperbenzoic acid; 1.) -78 deg C, 1 h, 2.) r.t., 4 h
View Scheme
参考文献
Minami, Toru; Hirakawa, Kazunari; Koyanagi, Shinichiro; Nakamura, Seigo; Yamaguchi, Masahiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2385 - 2390
