2,9-二羟甲基-1,10-菲啰啉合成路线 （共 6 条）
反应条件
sodium tetrahydroborate
Reduction; 4 h; Heating;
参考文献
Shaul, Mazi; Cohen, Yoram
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9358 - 9364
反应条件
sodium tetrahydroborate in ethylene glycol dimethyl ether
T=20°C; 8 h;
参考文献
Esposito, Veronica; Galeone, Aldo; Mayol, Luciano; Oliviero, Giorgia; Randazzo, Antonio; Varra, Michela
European Journal of Organic Chemistry, 2002 , # 24 p. 4228 - 4233
反应条件
1: SeO2 / dioxane / 3 h / Heating
2: NaBH4 / ethanol / Heating
View Scheme
参考文献
Goswami, Shyamaprosad; Mukherjee, Reshmi; Ray, Jayanta
Organic Letters, 2005 , vol. 7, # 7 p. 1283 - 1285
反应条件
1: 98 percent / pyridine; dimethylformamide / 12 h / 20 °C
2: NaBH4 / 1,2-dimethoxy-ethane / 8 h / 20 °C
View Scheme
参考文献
Esposito, Veronica; Galeone, Aldo; Mayol, Luciano; Oliviero, Giorgia; Randazzo, Antonio; Varra, Michela
European Journal of Organic Chemistry, 2002 , # 24 p. 4228 - 4233
反应条件
thionyl chloride
T=0°C; 2 h;
参考文献
Weijnen, John G. J.; Engbersen, Johan F. J.
Recueil des Travaux Chimiques des Pays-Bas, 1993 , vol. 112, p. 351 - 357
反应条件
hydrogen bromide
2 h; Heating;
参考文献
Chandler, Christopher J.; Deady, Leslie W.; Reiss, James A.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 599 - 602
