Thysanolactone合成路线 （共 8 条）
反应条件
in tetrahydrofuran
T=-18°C;
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
反应条件
1: 92 percent / PCC
2: 50 percent / tetrahydrofuran / -18 °C
View Scheme
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
反应条件
1: NBS, benzoyl peroxide
2: 47 percent / OsO4
3: Pb(OAc)4
4: CF3COOAg / acetonitrile; H2O
5: 81 percent / PCC
6: 74 percent / LiOH
7: 92 percent / PCC
8: 50 percent / tetrahydrofuran / -18 °C
View Scheme
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
反应条件
1: 47 percent / OsO4
2: Pb(OAc)4
3: CF3COOAg / acetonitrile; H2O
4: 81 percent / PCC
5: 74 percent / LiOH
6: 92 percent / PCC
7: 50 percent / tetrahydrofuran / -18 °C
View Scheme
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
反应条件
1: Pb(OAc)4
2: CF3COOAg / acetonitrile; H2O
3: 81 percent / PCC
4: 74 percent / LiOH
5: 92 percent / PCC
6: 50 percent / tetrahydrofuran / -18 °C
View Scheme
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
反应条件
1: 81 percent / PCC
2: 74 percent / LiOH
3: 92 percent / PCC
4: 50 percent / tetrahydrofuran / -18 °C
View Scheme
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
反应条件
1: CF3COOAg / acetonitrile; H2O
2: 81 percent / PCC
3: 74 percent / LiOH
4: 92 percent / PCC
5: 50 percent / tetrahydrofuran / -18 °C
View Scheme
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
反应条件
1: 74 percent / LiOH
2: 92 percent / PCC
3: 50 percent / tetrahydrofuran / -18 °C
View Scheme
参考文献
Aimi, Norio; Kawada, Kazuhiro; Sakai, Shin-ichiro
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 10 p. 3765 - 3768
