N-[(2-甲氧基苯基)甲基]-4-[4-(2-甲基苯基)哌嗪-1-基]苯胺合成路线 （共 5 条）
反应条件
hydrazine hydrate; palladium on activated charcoal in N,N-dimethyl-formamide
12 h; Heating;
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 512 - 514
反应条件
1: 70 percent / 48 h / 120 - 140 °C
2: 75 percent / hydrazin hydrate (98 percent) / Raney nickel / dimethylformamide / 10 h / Heating
3: 70 percent / benzene / 8 h / Heating
4: 55 percent / hydrazin hydrate (98 percent) / Pd-C (10 percent) / dimethylformamide / 12 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 512 - 514
反应条件
1: 70 percent / 48 h / 120 - 140 °C
2: 75 percent / hydrazin hydrate (98 percent) / Raney nickel / dimethylformamide / 10 h / Heating
3: 70 percent / benzene / 8 h / Heating
4: 55 percent / hydrazin hydrate (98 percent) / Pd-C (10 percent) / dimethylformamide / 12 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 512 - 514
反应条件
1: 70 percent / benzene / 8 h / Heating
2: 55 percent / hydrazin hydrate (98 percent) / Pd-C (10 percent) / dimethylformamide / 12 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 512 - 514
反应条件
1: 75 percent / hydrazin hydrate (98 percent) / Raney nickel / dimethylformamide / 10 h / Heating
2: 70 percent / benzene / 8 h / Heating
3: 55 percent / hydrazin hydrate (98 percent) / Pd-C (10 percent) / dimethylformamide / 12 h / Heating
View Scheme
参考文献
Agarwal, Jagdish C.; Gupta, Y. K.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 512 - 514
