(2-甲氧基苯基)-邻甲苯胺合成路线 （共 7 条）
反应条件
biphenyl-2-yl-di-tert-butyl-phosphane; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium (0) in toluene
T=20°C; Arylation; 23 h;
参考文献
Wolfe, John P.; Tomori, Hiroshi; Sadighi, Joseph P.; Yin, Jingjun; Buchwald, Stephen L.
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1158 - 1174
反应条件
tris(dibenzylideneacetone)dipalladium (0); X-Phos; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
T=150°C; 0.25 h; microwave irradiation;
参考文献
Tundel, Rachel E.; Anderson, Kevin W.; Buchwald, Stephen L.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 430 - 433
反应条件
tris-(dibenzylideneacetone)dipalladium(0); BI-DIME; sodium t-butanolate in m-xylene
T=130°C; Inert atmosphere;
参考文献
Rodriguez, Sonia; Qu, Bo; Haddad, Nizar; Reeves, Diana C.; Tang, Wenjun; Lee, Heewon; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 533 - 537
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
0.333333 h; Ambient temperature;
参考文献
Ohta; Miyata; Hirobe
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1221 - 1230
反应条件
copper diacetate in dichloromethane
4 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Donnelly, Dervilla, M. X.; Finet, Jean-Pierre; Guiry, Patrick J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 9 p. 2095 - 2102
反应条件
1: 19 percent / anhydrous K2CO3, Cu, I2 / 28 h / 200 °C
2: 44.3 percent / LiAlH4 / tetrahydrofuran / 0.33 h / Ambient temperature
View Scheme
参考文献
Ohta; Miyata; Hirobe
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1221 - 1230
反应条件
1: 19 percent / anhydrous K2CO3, Cu, I2 / 28 h / 200 °C
2: 44.3 percent / LiAlH4 / tetrahydrofuran / 0.33 h / Ambient temperature
View Scheme
参考文献
Ohta; Miyata; Hirobe
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1221 - 1230
