phosphorus pentachloride in neat (no solvent) 1.) 110-120 deg C, 1 h, 2.) room temp., 2.5 h then 90 deg C, 3 h; Title compound not separated from byproducts;
参考文献
Mahajan; Araujo
Canadian Journal of Chemistry, 1987 , vol. 65, # 1 p. 224 - 225
acetic anhydride; hydroquinone in chlorobenzene T=130°C; 8 h; in He;
参考文献
Mustafaev, A. M.; Alekperov, N. A.; Guseinov, M. M.; Imamaliev, A. B.; Mekhtiev, S. I.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1546 - 1552
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1691 - 1696
Komarov, N. V.; Lisovin, E. G.; Komarov, A. N.; Chekhun, A. L.; Kul'nevich, V. G.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 8 p. 1862 - 1865,1651 - 1653