1,1-二氯-2,2-二氟乙烯合成路线 （共 150 条）
反应条件
trihydrosilane P=4 Torr; Irradiationwave length 1033.5 cm-1, ratio SiH4/C2Cl2F2 = 3.0; MechanismProduct distribution;
参考文献
Pola, Josel; Simeonov, Sawa
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 1 p. 101 - 108
反应条件
aluminium trichloride T=20 - 25°C; 12 h; Yield given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 37, p. 151 - 170
反应条件
aluminium trichloride; monofluoro-trichloromethane
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 31, p. 3584 - 3592
反应条件
(i) di-n-butylammonium picrate, (ii) KOtBu, tBuOH; Multistep reaction;
参考文献
Bartlett,P.D. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 2049 - 2056
参考文献
Miller,W.T. et al.
Journal of the American Chemical Society, 1964 , vol. 86, p. 51 - 56
反应条件
sulfur(IV) fluoride; lead dioxide
T=100°C; 2 h;
参考文献
Bissell,E.R.; Fields,D.B.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1591 - 1593
反应条件
trifluoromethyl hypofluorite
T=-150 - 22°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Johri, Kamalesh K.; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 242 - 250
反应条件
T=-150 - 22°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Santos Afonso, M. dos; Czarnowski, J.
Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), 1988 , vol. 158, p. 25 - 34
反应条件
n-butyllithium
1.) ether, -70 deg C; 2.) -70 deg C, 1 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Okano, T.; Ito, K.; Kodaira, K.; Hosokawa, K.; Nishida, M.; et al.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 139 - 152
反应条件
n-butyllithium
1.) ether, -70 deg C; 2.) -70 deg C, 1 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Okano, T.; Ito, K.; Kodaira, K.; Hosokawa, K.; Nishida, M.; et al.
Journal of Fluorine Chemistry, 1988 , vol. 38, p. 139 - 152
