1,1-二氯-2,2-二氟乙烯合成路线 (共 150 条)
反应条件
Irradiation (UV/VIS); 240 h in vac.;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.2, page 81 - 87
反应条件
in dichloromethane
5 h; Irradiation;
参考文献
Okano, Takashi; Takakura, Nobuyuki; Nakano, Yuko; Okajima, Asako; Eguchi, Shoji
Tetrahedron, 1995 , vol. 51, # 7 p. 1903 - 1920
反应条件
trihydrosilane
P=5 Torr; Irradiationwave length 1033.5 cm-1, ratio SiH4/C2Cl2F2 = 9.6; MechanismProduct distribution;
参考文献
Pola, Josel; Simeonov, Sawa
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 1 p. 101 - 108
反应条件
trihydrosilane
P=5 Torr; Irradiationwave length 944.2 cm-1, ratio SiH4/C2Cl2F2 = 9.0; MechanismProduct distribution;
参考文献
Pola, Josel; Simeonov, Sawa
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 1 p. 101 - 108
参考文献
Masure,D. et al.
Synthesis, 1978 , p. 458 - 460
参考文献
Dedek,V. et al.
Collection of Czechoslovak Chemical Communications, 1978 , vol. 43, p. 985 - 997
反应条件
in acetonitrile
Ambient temperatureIrradiation;
参考文献
Okano, Takashi; Takakura, Nobuyuki; Nakano, Yuko; Okajima, Asako; Eguchi, Shoji
Tetrahedron, 1995 , vol. 51, # 7 p. 1903 - 1920
反应条件
n-butyllithium in diethyl ether
1 h; Heating;
参考文献
Kodaira, Kazuo; Okuhara, Kunio
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 5 p. 1625 - 1632
反应条件
n-butyllithium
Yield given. Yields of byproduct given;
参考文献
Okuhara, K.; Kodaira, K.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 497
参考文献
Dolbier, William R.; Burkholder, Conrad R.
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2381 - 2386