3-氯-1,1,2,3,3-五氟-1-丙烯合成路线 （共 19 条）
参考文献
Cirkva, Vladimir; Paleta, Oldrich; Ameduri, Bruno; Boutevin, Bernard
Journal of Fluorine Chemistry, 1995 , vol. 75, # 1 p. 87 - 92
反应条件
potassium fluoride; base
参考文献
Paleta, O.; Kvicala, J.; Dedek, V.
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 105
反应条件
acetone; sodium iodide
参考文献
Miller et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 4159,4163
参考文献
Miller
Patent: US2664449 , 1947 ;
参考文献
Miller
Nation.Nuclear Energy, Ser.Abt.VII Bd.1<1951>567,667
反应条件
potassium fluoride; base
参考文献
Paleta, O.; Kvicala, J.; Dedek, V.
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 105
反应条件
triethyl amine hydrochloride in diethylene glycol dimethyl ether
T=0 - 10°C; 2 h; Reagent/catalystSolvent;
参考文献
Daikin Industries, Ltd.; OHSHITA Shinsuke; HASHIKAWA Yuichi; KONDO Masahiro; YOSHIMURA Takashi; SHINOKI Noriyuki; Mantani, Emi
Patent: EP2554530 A1, 2013 ;
Location in patent: Paragraph 0066 ;
反应条件
hydrogen fluoride; metal oxide catalyst with 95atom percent chromium and 5atom percent zinc prepared by co-precipitation of zinc and chromium hydroxides, calcined at 900C, treated with HF at 175-400C
T=300°C; P=760.051 Torr; 0.00833333 h;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2008/60612 A2, 2008 ;
Location in patent: Page/Page column 17 ;
反应条件
phosphorous acid trisdiethylamide in benzonitrile
ice-salt bath;
参考文献
Montanari, Vittorio; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 5018 - 5019
反应条件
phosphorous acid trisdiethylamide in benzonitrile
ice-salt bath;
参考文献
Montanari, Vittorio; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 5018 - 5019
