反应条件
1.1: sodium hydride / diethyl ether / 2 h 1.2: 62 h 2.1: lithium aluminium tetrahydride / diethyl ether / -78 - 20 °C 3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve 4.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C 5.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); isopropylamine / 3.5 h 6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C 7.1: zinc / water; isopropyl alcohol / 26 h / 40 °C View Scheme
参考文献
McLean, Neville J.; Gansmuller, Axel; Concistre, Maria; Brown, Lynda J.; Levitt, Malcom H.; Brown, Richard C.D.
Tetrahedron, 2011 , vol. 67, # 43 p. 8404 - 8410
