3-甲基-4-(2,6,6-三甲基-1-环己烯-1-基)-3-丁烯-2-酮合成路线 （共 2 条）
反应条件
sulfuric acid in hexane
T=-8 - 26°C; 0.0333333 h;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2004/41764 A1, 2004 ;
Location in patent: Page/Page column 10 ;
反应条件
1.1: n-butyllithium / hexane / 0.33 h / -78 °C / |Inert atmosphere
1.2: 2 h / -78 - 20 °C / |Inert atmosphere
2.1: N-butylamine / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere
View Scheme
参考文献
Bassolino, Giovanni; Sovdat, Tina; Liebel, Matz; Schnedermann, Christoph; Odell, Barbara; Claridge, Timothy D.W.; Kukura, Philipp; Fletcher, Stephen P.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2650 - 2658
