1: With diisobutylaluminium hydride in n-heptane; dichloromethane T=-20 - -15°C; 0.166667 h; 2: With hydrogenchloride; water in n-heptane; dichloromethane
参考文献
WYETH
Patent: WO2009/76571 A1, 2009 ;
Location in patent: Page/Page column 41 ;
WO 2009/076571 A1
1: With n-butyllithium in tetrahydrofuran; hexane T=-90°C; 0.5 h; 2: With boric acid trimethyl ester in tetrahydrofuran; hexane T=-100°C; 0.333333 h; 3: With hydrogenchloride in tetrahydrofuran; hexane T=-100 - 20°C;
参考文献
Friedman; Toyne; Goodby; Hird
Journal of Materials Chemistry, 2001 , vol. 11, # 11 p. 2759 - 2772
1: 1-benzofuran-5-carbonitrile With n-butyllithium in tetrahydrofuran; hexanes T=-78°C; 0.5 h; 2: boric acid trimethyl ester in tetrahydrofuran; hexanes 0.333333 h; 3: With hydrogenchloride; water in tetrahydrofuran; hexanes 0.5 h;
