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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
79011-27-1
合成路线
（共 15 条）
79011-27-1
→
反应条件
4965-09-7
1-甲基-1,2,3,4-四氢异喹啉
反应条件
sodium hydroxide in ethanol 5 h; Heating;
参考文献
Shinohara, Tatsumi; Takeda, Akira; Toda, Jun; Terasawa, Noriyo; Sano, Takehiro
Heterocycles, 1997 , vol. 46, # 1 p. 555 - 565
205596-54-9
→
反应条件
79011-27-1
反应条件
sodium tetrahydroborate; nickel dichloride in tetrahydrofuran; methanol 0.5 h; Ambient temperature;
参考文献
Shinohara, Tatsumi; Takeda, Akira; Toda, Jun; Terasawa, Noriyo; Sano, Takehiro
Heterocycles, 1997 , vol. 46, # 1 p. 555 - 565
848772-46-3
→
反应条件
反应条件
tri-n-butyl-tin hydride; 1,1'-azobis (cyclohexanecarbonitrile) in toluene 1 h; Heating;
参考文献
Taniguchi, Tsuyoshi; Ishita, Atsuko; Uchiyama, Masahiko; Tamura, Osamu; Muraoka, Osamu; Tanabe, Genzoh; Ishibashi, Hiroyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1922 - 1925
848772-44-1
→
反应条件
79011-27-1
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 / 0 °C 2: 81 percent / NaHCO3 / xylene / 14 h / Heating 3: Bu3SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 1 h / Heating View Scheme
参考文献
Taniguchi, Tsuyoshi; Ishita, Atsuko; Uchiyama, Masahiko; Tamura, Osamu; Muraoka, Osamu; Tanabe, Genzoh; Ishibashi, Hiroyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1922 - 1925
848772-42-9
→
反应条件
79011-27-1
反应条件
1: 91 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; N-methylmorpholine / CH2Cl2 / 2 h / 0 °C 2: m-chloroperbenzoic acid / CH2Cl2 / 0 °C 3: 81 percent / NaHCO3 / xylene / 14 h / Heating 4: Bu3SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 1 h / Heating View Scheme
参考文献
Taniguchi, Tsuyoshi; Ishita, Atsuko; Uchiyama, Masahiko; Tamura, Osamu; Muraoka, Osamu; Tanabe, Genzoh; Ishibashi, Hiroyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1922 - 1925
848772-85-0
→
反应条件
79011-27-1
反应条件
1: 81 percent / NaHCO3 / xylene / 14 h / Heating 2: Bu3SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 1 h / Heating View Scheme
参考文献
Taniguchi, Tsuyoshi; Ishita, Atsuko; Uchiyama, Masahiko; Tamura, Osamu; Muraoka, Osamu; Tanabe, Genzoh; Ishibashi, Hiroyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1922 - 1925
848772-40-7
→
反应条件
79011-27-1
反应条件
1.1: BH3*THF / tetrahydrofuran / 1.5 h / Heating 1.2: 82 percent / I2 / tetrahydrofuran; methanol / 20 °C 2.1: 91 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; N-methylmorpholine / CH2Cl2 / 2 h / 0 °C 3.1: m-chloroperbenzoic acid / CH2Cl2 / 0 °C 4.1: 81 percent / NaHCO3 / xylene / 14 h / Heating 5.1: Bu3SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 1 h / Heating View Scheme
参考文献
Taniguchi, Tsuyoshi; Ishita, Atsuko; Uchiyama, Masahiko; Tamura, Osamu; Muraoka, Osamu; Tanabe, Genzoh; Ishibashi, Hiroyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1922 - 1925
18698-97-0
邻溴苯乙酸
→
反应条件
79011-27-1
反应条件
1.1: 74 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH2Cl2 / 20 °C 2.1: BH3*THF / tetrahydrofuran / 1.5 h / Heating 2.2: 82 percent / I2 / tetrahydrofuran; methanol / 20 °C 3.1: 91 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; N-methylmorpholine / CH2Cl2 / 2 h / 0 °C 4.1: m-chloroperbenzoic acid / CH2Cl2 / 0 °C 5.1: 81 percent / NaHCO3 / xylene / 14 h / Heating 6.1: Bu3SnH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene / 1 h / Heating View Scheme
参考文献
Taniguchi, Tsuyoshi; Ishita, Atsuko; Uchiyama, Masahiko; Tamura, Osamu; Muraoka, Osamu; Tanabe, Genzoh; Ishibashi, Hiroyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 5 p. 1922 - 1925
23069-99-0
N-(2-苯基乙基)-甲酰胺
+
75-07-0
乙醛
→
反应条件
79011-27-1
反应条件
acetic acid; trifluoroacetic acid 5 h; Heating;
参考文献
Lukanov, Ludmil K.; Venkov, Athanas P.; Mollov, Nikola M.
Synthesis, 1987 , # 11 p. 1031 - 1032
98-86-2
苯乙酮
→
反应条件
79011-27-1
反应条件
1: (isoPrO)4Ti / 3 h / 80 °C 2: NaBH4 / methanol / 1 h / Ambient temperature 3: 98 percent / Ac2O / 1 h / 70 °C 4: 93 percent / NaIO4 / H2O; methanol / Ambient temperature 5: 1.) TFAA; 2.) BF3*Et2O / 1.) benzene, RT, 1 h; 2.) benzene, RT, 1 h 6: 85 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Shinohara, Tatsumi; Takeda, Akira; Toda, Jun; Terasawa, Noriyo; Sano, Takehiro
Heterocycles, 1997 , vol. 46, # 1 p. 555 - 565
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