sodium tetrahydroborate in ethylene glycol dimethyl ether; water T=-15°C; Inert atmosphere;
参考文献
Rapireddy, Srinivas; Nhon, Linda; Meehan, Robert E.; Franks, Jonathan; Stolz, Donna Beer; Tran, Dat; Selsted, Michael E.; Ly, Danith H.
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4041 - 4044
1: 2-aminoisovaleric acid With lithium aluminium tetrahydride in tetrahydrofuran Reflux; 2: With sodium hydroxide in tetrahydrofuran; water 3: di-tert-butyl dicarbonate in tetrahydrofuran; water
参考文献
Bioorganic and Medicinal Chemistry, , vol. 17, # 13 p. 4486 - 4495