Aitken, R. Alan; Cowley, Alan H.; Gabbai, Francois P.; Masamba, Wayiza
Phosphorus, Sulfur and Silicon and the Related Elements, 1996 , vol. 111, p. 182
in tetrahydrofuran
under N2, addn. at 0°C, stirred for 4 h at 20°C; evapn. of volatiles, residue dissolved in petroleum ether, filtration, filtrate concd., crystn. at -28°C, recrystn. (petroleum ether); elem. anal.;
in tetrahydrofuran
under N2, addn. at 0°C, stirred for 4 h at 20°C; evapn. of volatiles, residue dissolved in petroleum ether, filtration, filtrate concd., crystn. at -28°C, recrystn. (petroleum ether); elem. anal.;
in tetrahydrofuran
under N2, addn. of C6H2(C(CH3)3)3PCl2 at 0°C to a soln. of (C5(CH3)5)(CO)(NO)ReP(Si(CH3)3)2, stirred for 30 min at 0°C; not isolated, detected by (31)P-NMR and IR-spectroscopy;
