N,N-二乙基-4-羟基苯甲酰胺合成路线 （共 21 条）
反应条件
potassium hydroxide
10 h; Heating;
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Stepanova, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 6 p. 1115 - 1119
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1287 - 1291
参考文献
Robertson, Jeffrey M.; Contreras, Cristina G.; Bates, Robert B.; Hall
Macromolecules, 2011 , vol. 44, # 14 p. 5586 - 5589
反应条件
1: pyridine / 0 °C / Inert atmosphere
2: N-butylamine / 1 h
3: 3 h / 120 °C
View Scheme
参考文献
Robertson, Jeffrey M.; Contreras, Cristina G.; Bates, Robert B.; Hall
Macromolecules, 2011 , vol. 44, # 14 p. 5586 - 5589
反应条件
1: thionyl chloride; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere
2: pyridine / 0 °C / Inert atmosphere
3: N-butylamine / 1 h
4: 3 h / 120 °C
View Scheme
参考文献
Robertson, Jeffrey M.; Contreras, Cristina G.; Bates, Robert B.; Hall
Macromolecules, 2011 , vol. 44, # 14 p. 5586 - 5589
反应条件
1: 36 percent / 4 h / 195 - 215 °C
2: 48 percent / 10percent aq. KOH / 10 h / Heating
View Scheme
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Stepanova, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 6 p. 1115 - 1119
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1287 - 1291
反应条件
benzene
Behandeln des Reaktionsprodukts mit wss. Natronlauge;
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
反应条件
aluminium trichloride
T=175 - 180°C; 3 h; changing amount of catalyst, temperature, and time; Product distribution;
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Stepanova, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 6 p. 1115 - 1119
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1287 - 1291
反应条件
aluminium trichloride
3 h; Heating; Product distribution;
参考文献
Isakova, A. P.; Naumov, Yu. A.; Nikeryasova, S. V.; Stepanova, A. A.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 6 p. 1115 - 1119
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1287 - 1291
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
反应条件
1: dibutyl ether; diethyl ether / Erhitzen des vom Diaethylaether befreiten Reaktionsgemisches auf Siedetemperatur und anschliessende Hydrolyse
3: sodium; ethanol
View Scheme
参考文献
Couturier
Annales de Chimie (Cachan, France), 1938 , vol. <11> 10, p. 559,597
