in dichloromethane
refluxing of (CH3C5H4)2TiCl2 in CH2Cl2 with phenylhydrazinium phenyldithiocarbazate for 8-10 h; hot filtration;; concn. in vac.; addn. of petroleum ether (60-80°C); storing overnight; crystallization; filtration; drying at 50°C for 2 h in vac.; elem. anal.;;
参考文献
Kaushik, N. K.; Bhushan, B.; Sodhi, G. S.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1981 , vol. 20, # 6 p. 625 - 626
