4-苯基-2,8-二氮杂螺[4.5]-3-癸酮合成路线 （共 5 条）
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol; water T=40°C;
参考文献
Parys, Marc Van; Vandewalle, Maurits
Bulletin des Societes Chimiques Belges, 1981 , vol. 90, # 7 p. 757 - 766
反应条件
1: sodium ethoxide / ethanol / 3 h / Heating 2: 80 percent / tetramethylguanidine / 168 h / Ambient temperature 3: 70 percent / hydrogen / Raney-nickel / methanol / 150 °C / 76000.1 Torr 4: 75 percent / hydrogen, 2 N hydrochloric acid / 10percent Pd/C / ethanol; H2O / 40 °C View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 90, # 7 p. 757 - 766
反应条件
1: sodium ethoxide / ethanol / 3 h / Heating 2: 80 percent / tetramethylguanidine / 168 h / Ambient temperature 3: 70 percent / hydrogen / Raney-nickel / methanol / 150 °C / 76000.1 Torr 4: 75 percent / hydrogen, 2 N hydrochloric acid / 10percent Pd/C / ethanol; H2O / 40 °C View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 90, # 7 p. 757 - 766
反应条件
1: 80 percent / tetramethylguanidine / 168 h / Ambient temperature 2: 70 percent / hydrogen / Raney-nickel / methanol / 150 °C / 76000.1 Torr 3: 75 percent / hydrogen, 2 N hydrochloric acid / 10percent Pd/C / ethanol; H2O / 40 °C View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 90, # 7 p. 757 - 766
反应条件
1: 70 percent / hydrogen / Raney-nickel / methanol / 150 °C / 76000.1 Torr 2: 75 percent / hydrogen, 2 N hydrochloric acid / 10percent Pd/C / ethanol; H2O / 40 °C View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 90, # 7 p. 757 - 766
