乙基(2R,4S)-4-甲基哌可酸酯合成路线 （共 5 条）
反应条件
10 palladium hydroxide on charcoal; hydrogen in ethanol
T=20°C; P=760.051 Torr; 4 h;
参考文献
Ferraboschi, Patrizia; Mieri, Maria De; Grisenti, Paride; Lotz, Matthias; Nettekoven, Ulrike
Tetrahedron Asymmetry, 2011 , vol. 22, # 16-17 p. 1626 - 1631
反应条件
hydrogen; palladium hydroxide - carbon in ethanol
P=760 Torr; Ambient temperature;
参考文献
Bailey, Patrick D.; Wilson, Robert D.; Brown, George R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1337 - 1340
反应条件
1: H2 / 3percent Pt-C / ethyl acetate / 16 h / 760 Torr / Ambient temperature
2: H2 / Pd(OH)2-C / ethanol / 760 Torr / Ambient temperature
View Scheme
参考文献
Bailey, Patrick D.; Wilson, Robert D.; Brown, George R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1337 - 1340
反应条件
1: TFA, H2O / dimethylformamide / 30 h / Ambient temperature
2: H2 / 3percent Pt-C / ethyl acetate / 16 h / 760 Torr / Ambient temperature
3: H2 / Pd(OH)2-C / ethanol / 760 Torr / Ambient temperature
View Scheme
参考文献
Bailey, Patrick D.; Wilson, Robert D.; Brown, George R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1337 - 1340
反应条件
1: 3 platinum on carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr
2: 10 palladium hydroxide on charcoal; hydrogen / ethanol / 4 h / 20 °C / 760.05 Torr
View Scheme
参考文献
Ferraboschi, Patrizia; Mieri, Maria De; Grisenti, Paride; Lotz, Matthias; Nettekoven, Ulrike
Tetrahedron Asymmetry, 2011 , vol. 22, # 16-17 p. 1626 - 1631
