Smith, Mark E.B.; Derrien, Nadine; Lloyd, Michael C.; Taylor, Stephen J.C.; Chaplin, David A.; McCague, Raymond
Tetrahedron Letters, 2001 , vol. 42, # 7 p. 1347 - 1350
1: Oxone / H2O / 7 h / pH 6 2: 67 percent / DMAP / CH2Cl2 / 5 h / 0 - 20 °C 3: 100 percent / NaOMe / methanol / 16 h / 0 - 20 °C 4: H2 / [(COD)py(PCy3)]PF6 / methanol / 14 h View Scheme
参考文献
Smith, Mark E.B.; Derrien, Nadine; Lloyd, Michael C.; Taylor, Stephen J.C.; Chaplin, David A.; McCague, Raymond
Tetrahedron Letters, 2001 , vol. 42, # 7 p. 1347 - 1350
1: 1.264 g / tetrahydrofuran; H2O / 18 h / 20 - 60 °C 2: 90.5 percent / LiAlH4 / tetrahydrofuran / 19.5 h / 0 °C / Heating 3: 83 percent / Et3N / ethanol / 7 h / Heating View Scheme
参考文献
Daluge, Susan M.; Martin, Michael T.; Sickles, Barry R.; Livingston, Douglas A.
Nucleosides, Nucleotides and Nucleic Acids, 2000 , vol. 19, # 1-2 p. 297 - 327
