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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
79213-82-4
合成路线
（共 10 条）
6317-85-7
4-(二甲氨基)安息香
→
反应条件
79213-82-4
反应条件
1: 80.4 percent / HCl(g) / H2O / 48 h / Ambient temperature 2: Et3N, NH4OAc / methanol / 5 h / 45 °C View Scheme
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
33458-29-6
+
67-64-1
丙酮
→
反应条件
99052-55-8
反应条件
ammonium acetate; triethylamine in methanol T=45°C; 17 h; Further byproducts given;
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
33458-29-6
→
反应条件
99052-55-8
反应条件
ammonium acetate; triethylamine; acetone in methanol T=40°C; 2 h; Further byproducts given;
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
33458-29-6
→
反应条件
6317-85-7
4-(二甲氨基)安息香
+
99052-55-8
反应条件
ammonium acetate; triethylamine; acetone in butan-1-ol T=45°C; 7.5 h; Further byproducts given;
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
100-10-7
对二甲氨基苯甲醛
+
14491-02-2
→
反应条件
79213-82-4
反应条件
in 1,4-dioxane 1.5 h; Irradiation;
参考文献
Pfoertner; Bernauer; Kaufmann; Lorch
Helvetica Chimica Acta, 1985 , vol. 68, # 3 p. 584 - 591
33458-29-6
+
67-64-1
丙酮
→
反应条件
6317-85-7
4-(二甲氨基)安息香
反应条件
ammonium acetate; triethylamine in water T=45°C; 5 h; Further byproducts given;
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
33458-29-6
+
67-64-1
丙酮
→
反应条件
6317-85-7
4-(二甲氨基)安息香
+
99052-55-8
反应条件
ammonium acetate; triethylamine in methanol T=45°C; 5 h; Further byproducts given;
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
100-52-7
苯甲醛
→
反应条件
79213-82-4
反应条件
1: 61.9 percent / KCN / ethanol; H2O / 5 h / Heating 2: 80.4 percent / HCl(g) / H2O / 48 h / Ambient temperature 3: Et3N, NH4OAc / methanol / 5 h / 45 °C View Scheme
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
100-10-7
对二甲氨基苯甲醛
→
反应条件
79213-82-4
反应条件
1: 61.9 percent / KCN / ethanol; H2O / 5 h / Heating 2: 80.4 percent / HCl(g) / H2O / 48 h / Ambient temperature 3: Et3N, NH4OAc / methanol / 5 h / 45 °C View Scheme
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
33458-29-6
+
67-64-1
丙酮
→
反应条件
6317-85-7
4-(二甲氨基)安息香
反应条件
ammonium acetate; triethylamine in methanol T=45°C; 7.5 h; further solvent, time; Product distribution;
参考文献
Foricher, Joseph; Montavon, Francois; Pfoertner, Karl-Heinz; Schoenholzer, Peter
Helvetica Chimica Acta, 1985 , vol. 68, p. 592 - 599
