4-[(E)-丁-2-烯酰基]-3-甲氧基-5-甲基苯甲酸合成路线 (共 8 条)
反应条件
1: H2 / PtO2 / aq. ethanol / 2 h 2: 50percent aq. KOH / 0.5 h View Scheme
参考文献
Sato, Hiroji; Konoma, Keiichi; Sakamura, Sadao
Agricultural and Biological Chemistry, 1981 , vol. 45, # 7 p. 1675 - 1680
反应条件
macrophomate synthase; magnesium chloride
T=30°C; Condensation; rearrangement; 0.166667 h; Enzymatic reaction;
参考文献
Oikawa, Hideaki; Watanabe, Kenji; Yagi, Kenji; Ohashi, Satoshi; Mie, Takashi; Ichihara, Akitami; Honma, Mamoru
Tetrahedron Letters, 1999 , vol. 40, # 38 p. 6983 - 6986
反应条件
hydrogenchloride
13 h; Heating;
参考文献
Ichihara, Akitami; Murakami, Kazuo; Sakamura, Sadao
Agricultural and Biological Chemistry, 1984 , vol. 48, # 3 p. 833 - 834
反应条件
1: LDA / tetrahydrofuran
2: 47.4 percent / conc. aq. HCl / 13 h / Heating
View Scheme
参考文献
Ichihara, Akitami; Murakami, Kazuo; Sakamura, Sadao
Agricultural and Biological Chemistry, 1984 , vol. 48, # 3 p. 833 - 834
反应条件
dipotassium hydrogenphosphate; sodium dihydrogenphosphate in ethanol; water
480 h; fermentation process;
参考文献
Sakurai, Ikuo; Miyajima, Hisae; Akiyama, Katsuyoshi; Shimizu, Sakae; Yamamoto, Yuzuru
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 2003 - 2011
反应条件
dipotassium hydrogenphosphate; sodium dihydrogenphosphate in ethanol; water
480 h; fermentation process;
参考文献
Sakurai, Ikuo; Miyajima, Hisae; Akiyama, Katsuyoshi; Shimizu, Sakae; Yamamoto, Yuzuru
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, p. 2003 - 2011
反应条件
pyridine
Title compound not separated from byproducts;
参考文献
Sato, Hiroji; Konoma, Keiichi; Sakamura, Sadao
Agricultural and Biological Chemistry, 1981 , vol. 45, # 7 p. 1675 - 1680
反应条件
pyridine
Title compound not separated from byproducts;
参考文献
Sato, Hiroji; Konoma, Keiichi; Sakamura, Sadao
Agricultural and Biological Chemistry, 1981 , vol. 45, # 7 p. 1675 - 1680