1: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C 2: chlorotrimethylsilane / 18 h / Heating 3: tetrahydrofuran / 12 h 4: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C View Scheme

tert.-butylhydroperoxide; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in dichloromethane T=30°C; Title compound not separated from byproducts;

tert.-butylhydroperoxide; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in dichloromethane T=30°C; Title compound not separated from byproducts;