反应条件
1: With bis[2-(N,N-dimethylamino)ethyl] ether; isopropylmagnesium chloride in tetrahydrofuran T=15°C; 2: With boric acid trimethyl ester in tetrahydrofuran 0.666667 h; 3: With hydrogenchloride; water in tetrahydrofuran T=20°C; 2 h;
参考文献
BRISTOL-MYERS SQUIBB COMPANY; PURANDARE, Ashok, Vinayak; BATT, Douglas, G.; LIU, Qingjie; JOHNSON, Walter, L.; MASTALERZ, Harold; ZHANG, Guifen; ZIMMERMANN, Kurt
Patent: WO2010/80474 A1, 2010 ;
Location in patent: Page/Page column 172 ;
WO 2010/080474 A1