2,6-双[[双(2-吡啶甲基)氨基]甲基]-4-(2-萘)苯酚合成路线 （共 4 条）
反应条件
1: With potassium carbonate; potassium iodide in acetonitrile
12 h; Heating;
2: With sodium hydroxide in methanol
T=20°C; 4 h;
参考文献
Lee, Dong Hoon; Kim, Soon Young; Hong, Jong-In
Angewandte Chemie - International Edition, 2004 , vol. 43, # 36 p. 4777 - 4780
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane; water
Suzuki Coupling; 15 h; Inert atmosphereReflux;
参考文献
Pathberiya, L. Gayathri; Nguyen, Tran; Tuck, Kellie L.; Barlow, Nicholas; Graham, Bim
Tetrahedron, 2012 , vol. 68, # 46 p. 9435 - 9439,5
反应条件
1: water; isopropyl alcohol / 15 h / |Reflux
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; 1,4-dioxane / 15 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Pathberiya, L. Gayathri; Nguyen, Tran; Tuck, Kellie L.; Barlow, Nicholas; Graham, Bim
Tetrahedron, 2012 , vol. 68, # 46 p. 9435 - 9439,5
反应条件
1: water; isopropyl alcohol / 15 h / |Reflux
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; 1,4-dioxane / 15 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Pathberiya, L. Gayathri; Nguyen, Tran; Tuck, Kellie L.; Barlow, Nicholas; Graham, Bim
Tetrahedron, 2012 , vol. 68, # 46 p. 9435 - 9439,5
