di(n-butyl)tin oxide in 1,3,5-trimethyl-benzene
19 h; Heating;
参考文献
Steliou, Kosta; Szczygielska-Nowosielska, A.; Favre, A.; Poupart, M.A.; Hanessian, Stephen
Journal of the American Chemical Society, 1980 , vol. 102, # 25 p. 7578 - 7579
1: With bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in dichloromethane
24 h; Heating;
2: With hydrogen; palladium on activated charcoal in ethyl acetate
T=20°C; 6 h; Further stages. Title compound not separated from byproducts.;
1: With caesium carbonate in ethanol
2: With Merryfield resin in N,N-dimethyl-formamide
T=50°C; 72 h;
3: With di(n-butyl)tin oxide in chlorobenzene
T=133°C; 18 h; Further stages. Further byproducts. Title compound not separated from byproducts.;
参考文献
Ruddick, Clare L.; Hodge, Philip; Cook, Anthony; McRiner, Andrew J.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 5 p. 629 - 637
