1: 2-bromo-9,9-dihexyl-9-H-fluorene With n-butyllithium in diethyl ether; hexane
T=-78 - 20°C;
2: N,N-dimethyl-formamide in diethyl ether; hexane
T=20°C; 20 h; Further stages.;
参考文献
Barker, Carl A.; Zeng, Xianshun; Bettington, Sylvia; Batsanov, Andrei S.; Bryce, Martin R.; Beeby, Andrew
Chemistry - A European Journal, 2007 , vol. 13, # 23 p. 6710 - 6717