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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
793706-87-3
合成路线
(共 11 条)
100-52-7
苯甲醛
+
793706-87-3
→
反应条件
1885-38-7
肉桂腈
+
24840-05-9
反应条件
potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
1121-60-4
吡啶-2-甲醛
+
793706-87-3
→
反应条件
反应条件
potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
100-52-7
苯甲醛
+
793706-87-3
→
反应条件
24840-05-9
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; Peterson reaction; 3 h;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
100-52-7
苯甲醛
+
793706-87-3
→
反应条件
1885-38-7
肉桂腈
+
24840-05-9
反应条件
potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
630-19-3
特戊醛
+
793706-87-3
→
反应条件
29582-19-2
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
135-02-4
2-甲氧基苯甲醛
+
793706-87-3
→
反应条件
反应条件
potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
98-01-1
糠醛
+
793706-87-3
→
反应条件
6137-73-1
+
6125-63-9
(E)-3-(2-呋喃)丙烯腈
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
98-01-1
糠醛
+
793706-87-3
→
反应条件
6137-73-1
反应条件
potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; Peterson reaction; 3 h;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
98-01-1
糠醛
+
793706-87-3
→
反应条件
6137-73-1
+
6125-63-9
(E)-3-(2-呋喃)丙烯腈
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
89-98-5
2-氯苯甲醛
+
793706-87-3
→
反应条件
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=-78°C; Peterson reaction; 3 h; Title compound not separated from byproducts;
参考文献
Kojima, Satoshi; Fukuzaki, Tomohide; Yamakawa, Atsushi; Murai, Yutaka
Organic Letters, 2004 , vol. 6, # 22 p. 3917 - 3920
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