4-乙酰氨基-3-硝基吡啶合成路线 （共 7 条）
反应条件
dinitrogen pentaoxide in nitromethane T=0°C; Nitration; 0.166667 h;
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
1: 97 percent / Et3N / acetonitrile / 1 h / 20 °C 2: 72 percent / N2O5 / nitromethane / 0.17 h / 0 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 36, # 5 p. 1143 - 1145
参考文献
Pharmaceutical Bulletin, , vol. 2, p. 34,36
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; Hydrogenation; P=5250.42 Torr; 23 h;
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
1: 96 percent / 2 M aq. HCl / 5 h / 70 °C 2: 98 percent / H2 / 5 percent Pd/C / methanol / 20 h / 20 °C / 5250.42 Torr View Scheme
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
1: 97 percent / H2 / 5 percent Pd/C / methanol / 23 h / 20 °C / 5250.42 Torr 2: 97 percent / AcOH / 1.5 h / Heating View Scheme
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
hydrogenchloride T=70°C; Hydrolysis; 5 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 36, # 5 p. 1143 - 1145
