2-甲氧基-6-甲基苯甲酸甲酯合成路线 （共 20 条）
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 0.5 h; HeatingIrradiation;
参考文献
Ghera, E.; Plemenitas, A.; Ben-David, Y.
Synthesis, 1984 , # 6 p. 504 - 506
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetone Reflux;
参考文献
Senthilmnrugan, Annamalai; Aidhen, Indrapal Singh
European Journal of Organic Chemistry, 2010 , # 3 p. 555 - 564
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C; 16 h;
参考文献
Baur, Benjamin; Storch, Kirsten; Martz, Kathrin E.; Goettert, Marcia I.; Richters, Andre; Rauh, Daniel; Laufer, Stefan A.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 21 p. 8561 - 8578
反应条件
in diethyl ether T=0°C; 2 h;
参考文献
Mandal, Samir Kumar; Roy, Subhas Chandra
Tetrahedron, 2008 , vol. 64, # 49 p. 11050 - 11057
反应条件
potassium carbonate in acetone
参考文献
Tyman, John H. P.; Visani, Naina
Journal of Chemical Research, Miniprint, 1997 , # 1 p. 228 - 240
反应条件
1: N-bromosuccinimide / azobisisobutyronitrile / CCl4 / 0.33 h / Heating; Irradiation 2: 1.) AgNO3, NaHCO3, 2.) triethylamine / 1.) DMSO, room temp, 1 h, 2.) 15 min 3: 71 percent / n-bromosuccinimide / azobisisobutyronitrile / CCl4 / 0.5 h / Heating; Irradiation View Scheme
参考文献
Synthesis, , # 6 p. 504 - 506
反应条件
1: 1.) AgNO3, NaHCO3, 2.) triethylamine / 1.) DMSO, room temp, 1 h, 2.) 15 min 2: 71 percent / n-bromosuccinimide / azobisisobutyronitrile / CCl4 / 0.5 h / Heating; Irradiation View Scheme
参考文献
Synthesis, , # 6 p. 504 - 506
反应条件
sulfuric acid in 1,2-dichloro-ethane 6 h; Heating;
参考文献
Islam, Md. Rabiul; Joule, John A.
Journal of Chemical Research, Miniprint, 1991 , # 2 p. 367 - 378
反应条件
1.1: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C 2.1: sulfuric acid; sodium nitrite / water / 0.5 h / 0 °C 2.2: 0.5 h / |Reflux 3.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 21 p. 8561 - 8578
反应条件
1.1: sulfuric acid; sodium nitrite / water / 0.5 h / 0 °C 1.2: 0.5 h / |Reflux 2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 70 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 21 p. 8561 - 8578
