2-甲氧基-6-甲基苯甲酸甲酯合成路线 （共 20 条）
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in hexane T=25°C; without TMEDA, other metallating agent, solvent and temperature; Product distribution;
参考文献
Tetrahedron, , vol. 39, # 12 p. 2031 - 2042
反应条件
1: 83 percent / SOCl2 / 4 h / Heating 2: 1.) Na / 2.) reflux, 2 h View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 2 p. 367 - 378
参考文献
Bulletin de la Societe Scientifique de Bretagne, , vol. 31, p. Sonderheft S.9,41
反应条件
sodium 2.) reflux, 2 h; Yield given. Multistep reaction;
参考文献
Journal of Chemical Research, Miniprint, , # 2 p. 367 - 378
反应条件
sodium hydrogencarbonate
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 1 p. 360 - 365
反应条件
(i) Li, hexane, Et2O, (ii) /BRN= 1900390/, (iii) /BRN= 102415/; Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 11, p. 209 - 216
反应条件
Yield given. Multistep reaction;
参考文献
Tarnchompoo; Thebtaranonth
Synthesis, 1986 , vol. NO. 9, p. 785 - 786
参考文献
Shirley,D.A. et al.
Journal of Organometallic Chemistry, 1968 , vol. 11, p. 209 - 216
反应条件
1: 57 percent / NBS, benzoyl peroxide / CCl4 / 6 h / Heating; Irradiation
2: CaCO3 / ethanol; H2O / Heating
View Scheme
参考文献
Islam, Md. Rabiul; Joule, John A.
Journal of Chemical Research, Miniprint, 1991 , # 2 p. 367 - 378
反应条件
1: 92 percent / NBS; AIBN / CCl4
2: 53 percent / Cp2TiCl2 / tetrahydrofuran / 20 °C
3: 88 percent / BBr3 / CH2Cl2 / -78 - 20 °C
View Scheme
参考文献
Mandal, Samir Kumar; Roy, Subhas Chandra
Tetrahedron Letters, 2007 , vol. 48, # 23 p. 4131 - 4134
