2-溴-3-甲基-2-丁酸乙酯合成路线 （共 6 条）
反应条件
triethylamine; phosphonic acid diethyl ester T=80°C; 30 h; Yield given. Yields of byproduct given;
参考文献
Hirao, Toshikazu; Fujihara, Yoshimi; Kurokawa, Ken; Ohshiro, Yoshiki; Agawa, Toshio
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2830 - 2832
反应条件
potassium carbonate in acetone T=45°C; 72 h; Yield given. Yields of byproduct given;
参考文献
Rosnati, Vittorio; Saba, Antonio; Salimbeni, Aldo; Vettori, Umberto
Gazzetta Chimica Italiana, 1981 , vol. 111, # 7/8 p. 249 - 256
反应条件
potassium carbonate in acetone
Heating;
参考文献
Babler; Invergo
Tetrahedron Letters, 1981 , vol. 22, # 29 p. 2743 - 2746
反应条件
1: Oxone(R); aq. HBr / CH2Cl2 / 2 h / 20 °C
2: Et3N / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Kim, Kyoung-Mahn; Park, In-Hwan
Synthesis, 2004 , # 16 p. 2641 - 2644
反应条件
triethylamine; phosphonic acid diethyl ester
T=80°C; 30 h; Yield given. Yields of byproduct given;
参考文献
Hirao, Toshikazu; Fujihara, Yoshimi; Kurokawa, Ken; Ohshiro, Yoshiki; Agawa, Toshio
Journal of Organic Chemistry, 1986 , vol. 51, # 14 p. 2830 - 2832
反应条件
potassium carbonate in acetone
T=45°C; 24 h; MechanismProduct distribution;
参考文献
Rosnati, Vittorio; Saba, Antonio; Salimbeni, Aldo; Vettori, Umberto
Gazzetta Chimica Italiana, 1981 , vol. 111, # 7/8 p. 249 - 256
