1,3,5-三甲基-1,3,5-环己烷三羧酸三基酯合成路线 （共 5 条）
反应条件
sodium hydroxide in methanol T=65°C; 12 h;
参考文献
Rebek,J.; Askew,B.; Killoran,M.
Journal of the American Chemical Society, 1987 , vol. 109, p. 2426
反应条件
lithium diisopropyl amide in diethyl ether
Ambient temperature; Yields of byproduct given;
参考文献
Rebek,J.; Askew,B.; Killoran,M.
Journal of the American Chemical Society, 1987 , vol. 109, p. 2426
反应条件
1: trimethyl cyclohexane-1,3,5-tricarboxylate With n-butyllithium; diisopropylamine in diethyl ether; hexane
T=0°C; 2 h;
2: dimethyl sulfate in diethyl ether; hexane
T=20°C;
参考文献
Ye, Qing; Komarov, Igor V.; Kirby, Anthony J.; Jones Jr., Maitland
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9288 - 9294
反应条件
1: trimethyl cis,cis-cyclohexane-1,3,5-tricarboxylate With lithium diisopropyl amide in diethyl ether
T=0°C; 2 h;
2: dimethyl sulfate in diethyl ether
T=20°C; 12 h;
参考文献
Chuang, Tsung-Hsun; Fang, Jim-Min
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 193 - 200
参考文献
Kemp, D. S.; Petrakis, Konstantinos S.
Journal of Organic Chemistry, 1981 , vol. 46, p. 5140 - 5143
