2,2-二甲基-4-己基-1,3-二氧杂烷合成路线 (共 8 条)
反应条件
C18-alkylated polystyrene-supported sulfonic acid; water T=40°C; 2 h;
参考文献
Iimura, Shinya; Manabe, Kei; Kobayashi, Shue
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 14 p. 2416 - 2418
反应条件
bismuth(III) chloride
1 h; Heating;
参考文献
Mohammadpoor-Baltork; Khosropour; Aliyan
Synthetic Communications, 2001 , vol. 31, # 22 p. 3411 - 3416
反应条件
chromyl nitrate in tetrachloromethane
T=-78°C; 1 h; Title compound not separated from byproducts;
参考文献
Miyaura, N.; Kochi, J. K.
Journal of the American Chemical Society, 1983 , vol. 105, # 8 p. 2368 - 2378
反应条件
iodine
Ambient temperature;
参考文献
Konaklieva; Dahl; Turos
Tetrahedron Letters, 1992 , vol. 33, # 47 p. 7093 - 7096
反应条件
iodine in acetone
Ambient temperature;
参考文献
Konaklieva; Dahl; Turos
Tetrahedron Letters, 1992 , vol. 33, # 47 p. 7093 - 7096
反应条件
pyridinium p-toluenesulfonate
T=20°C; 2 h; Inert atmosphere;
参考文献
Valerio, Viviana; Petkova, Desislava; Madelaine, Claire; Maulide, Nuno
Chemistry - A European Journal, 2013 , vol. 19, # 8 p. 2606 - 2610
反应条件
toluene-4-sulfonic acid; copper(II) sulfate
参考文献
Miyaura, N.; Kochi, J. K.
Journal of the American Chemical Society, 1983 , vol. 105, # 8 p. 2368 - 2378
反应条件
1: oct-1-ene With osmium(VIII) oxide; 4-methylmorpholine N-oxide
2: 2,2-dimethoxy-propane With toluene-4-sulfonic acid
参考文献
Schuster, Christopher H.; Li, Bo; Morken, James P.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 34 p. 7906 - 7909