(E)-3-(3-溴苯基)丙烯酸甲酯合成路线 （共 11 条）
反应条件
triethylamine in water; N,N-dimethyl-formamide T=90°C; Heck Reaction; 16 h;
参考文献
Pavia, Cinzia; Giacalone, Francesco; Bivona, Lucia Anna; Salvo, Anna Maria Pia; Petrucci, Chiara; Strappaveccia, Giacomo; Vaccaro, Luigi; Aprile, Carmela; Gruttadauria, Michelangelo
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 387, p. 57 - 62
参考文献
Beecham Group p.l.c.
Patent: US4713486 A1, 1987 ;
反应条件
hydrogenchloride 12 h;
参考文献
Ambler, Brett R.; Altman, Ryan A.
Organic Letters, 2013 , vol. 15, # 21 p. 5578 - 5581
反应条件
chromium dichloride in tetrahydrofuran T=20°C; 12 h;
参考文献
Barma, Deb K.; Kundu, Asish; Bandyopadhyay, Anish; Kundu, Abhijit; Sangras, Bhavani; Briot, Anne; Mioskowski, Charles; Falck
Tetrahedron Letters, 2004 , vol. 45, # 30 p. 5917 - 5920
参考文献
US6166006 A1, ;
US 6166006 A
反应条件
in methanol; ethyl acetate
参考文献
E. R. Squibb and Sons, Inc.
Patent: US5827868 A1, 1998 ;
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2 in methanol T=20°C; 2 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 11-12 p. 1923 - 1926
反应条件
1: diethyl methoxycarbonylmethyl-phosphonate With sodium hydride in tetrahydrofuran T=0 - 20°C; 2: 3-bromo-benzaldehyde in tetrahydrofuran; dichloromethane T=20°C;
参考文献
Journal of the American Chemical Society, , vol. 133, # 17 p. 6642 - 6649
反应条件
sodium tetrahydroborate; hydrogen; nickel diacetate in methanol; ethyl acetate T=20°C; P=1500.15 Torr; 0.333333 h;
参考文献
Erdelyi, Mate; Karlen, Anders; Gogoll, Adolf
Chemistry - A European Journal, 2006 , vol. 12, # 2 p. 403 - 412
反应条件
1: diisobutylaluminium hydride / dichloromethane / -78 °C 2: Dess-Martin periodane / dichloromethane / 20 °C View Scheme
参考文献
Kim, Eunha; Koh, Minseob; Lim, Byung Joon; Park, Seung Bum
Journal of the American Chemical Society, 2011 , vol. 133, # 17 p. 6642 - 6649
