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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
79482-22-7
合成路线
（共 13 条）
131223-44-4
→
反应条件
79482-22-7
反应条件
copper dichloride; dichloro bis(acetonitrile) palladium(II) in 1,2-dichloro-ethane T=25°C;
参考文献
Liu, Cong; Wang, Xiang; Pei, Tao; Widenhoefer, Ross A.
Chemistry - A European Journal, 2004 , vol. 10, # 24 p. 6343 - 6352
131223-44-4
→
反应条件
79482-22-7
反应条件
dichloro bis(acetonitrile) palladium(II); copper dichloride in 1,2-dichloro-ethane T=20°C;
参考文献
Pei, Tao; Wang, Xiang; Widenhoefer, Ross A.
Journal of the American Chemical Society, 2003 , vol. 125, # 3 p. 648 - 649
79482-32-9
→
反应条件
79482-22-7
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane Ambient temperature;
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
1262861-81-3
→
反应条件
79482-22-7
反应条件
zinc(II) chloride; ytterbium(III) triflate T=100°C; Conia-ene reaction; 24 h; Inert atmosphereneat (no solvent);
参考文献
Liu, Yu; Song, Ren-Jie; Li, Jin-Heng
Synthesis, 2010 , # 21 art. no. F10810SS, p. 3663 - 3669
1193-18-6
3-甲基-2-环己烯-1-酮
+
98-88-4
苯甲酰氯
→
反应条件
79482-22-7
反应条件
sodium tert-pentoxide in benzene 1 h; Ambient temperature;
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
98-88-4
苯甲酰氯
→
反应条件
79482-22-7
反应条件
1: pyridine / CHCl3 / 4 h / Ambient temperature 2: AlCl3 / 1,2-dichloro-ethane / 17 h / Ambient temperature 3: 76 percent / oxalyl chloride / 3 h / 0 °C 4: NaH / benzene / 2.5 h / 60 °C / Heating 5: p-TsOH / benzene / 10 h / Heating View Scheme
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
1193-18-6
3-甲基-2-环己烯-1-酮
→
反应条件
79482-22-7
反应条件
1: 60 percent / lithium dimethylcuprate / diethyl ether; hexamethylphosphoric acid triamide / 2 h / Ambient temperature 2: 58 percent / NaH (60percent) / tetrahydrofuran / Ambient temperature 3: 73 percent / m-CPBA / CH2Cl2 / Ambient temperature View Scheme
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
66049-39-6
→
反应条件
79482-22-7
反应条件
1: AlCl3 / 1,2-dichloro-ethane / 17 h / Ambient temperature 2: 76 percent / oxalyl chloride / 3 h / 0 °C 3: NaH / benzene / 2.5 h / 60 °C / Heating 4: p-TsOH / benzene / 10 h / Heating View Scheme
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
69629-50-1
2-苯甲酰基-1,3-环己二酮
→
反应条件
79482-22-7
反应条件
1: 76 percent / oxalyl chloride / 3 h / 0 °C 2: NaH / benzene / 2.5 h / 60 °C / Heating 3: p-TsOH / benzene / 10 h / Heating View Scheme
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
504-02-9
1,3-环己二酮
→
反应条件
79482-22-7
反应条件
1: pyridine / CHCl3 / 4 h / Ambient temperature 2: AlCl3 / 1,2-dichloro-ethane / 17 h / Ambient temperature 3: 76 percent / oxalyl chloride / 3 h / 0 °C 4: NaH / benzene / 2.5 h / 60 °C / Heating 5: p-TsOH / benzene / 10 h / Heating View Scheme
参考文献
Tamura, Yasumitsu; Wada, Akimori; Okuyama, Shigehiro; Fukumori, Satoshi; Hayashi, Yoko; et al.
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1312 - 1320
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